Thermal, Structural and Morphology Studies of PEO-LICF3SO3-DBP-ZrO2 Nanocomposite Polymer Electrolytes

Authors

  • Siti Mariah Faculty of Mechanical Engineering & Technology, University Malaysia Perlis
  • Mohd Rafie Johan Nanotechnology & Catalysis Research Centre (NANOCAT), Institute of Advanced Studies, University of Malaya

DOI:

https://doi.org/10.22452/mnij.vol1no1.1

Keywords:

Polymer electrolyte, Ionic conductivity, Thin films, Differential scanning calorimetry

Abstract

This work represents thermal study of PEO-based polymer electrolyte films that were prepared by the solution cast technique. The melting temperature Tm, glass transition temperature Tg and degree of crystallinity χc were measured by diffraction scanning calorimetry (DSC). Thermogravimetric (TGA) was used to determine the initial and final degradation temperatures. The structural was also performed to characterize the vibrational wavelength and phase characteristic (crystalline/amorphous). While the morphological study was emphasized to examine the features appearance for pure polymer electrolyte system as well as after addition salt, plasticizer and filler. The zirconium oxide particles were measured after the milling process by using the transmission electron microscopy (TEM), and the particles obtained in the range of 9 – 54 nanometer size.

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Thermal, Structural and Morphology Studies of PEO-LICF3SO3-DBP-ZrO2 Nanocomposite Polymer Electrolytes

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Published

25-08-2021

How to Cite

Mohd Yasin, S. M. ., & Johan, M. R. (2021). Thermal, Structural and Morphology Studies of PEO-LICF3SO3-DBP-ZrO2 Nanocomposite Polymer Electrolytes. Malaysian NANO-An International Journal, 1(1), 1–17. https://doi.org/10.22452/mnij.vol1no1.1